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May
2012
April
2012
March
2012

7th Solid-State NMR Workshop at CSC 2012 (May 16/12)

The National Ultrahigh-Field NMR Facility for Solids and Bruker Canada are pleased to present the 7th Annual Solid-State NMR Workshop at the 95th Canadian Chemistry Conference and Exhibition in Calgary (CSC 2012). The workshop will take place on Saturday, May 26, 2012, 13:00 - 19:00, in the Calgary TELUS Convention Centre.

This annual Canadian solid-state NMR event focuses on the latest developments in solid-state NMR spectroscopy with emphasis on practical aspects and applications in materials and life sciences. The workshop will be of interest not only to NMR spectroscopists, but also to students and other researchers interested in using modern NMR techniques in their research practice.

Download the Workshop Program and Abstracts (PDF)

Workshop program

Session 1 (CTCC, Chinook 4), Chair David Bryce (University of Ottawa)

13:00-13:05 David Bryce (University of Ottawa) Opening comments

13:05-13:25 Anne-Marie Thompson (NSERC) "Major Resources Support program" (brief presentation and discussion)

13:25-13:50 Roderick Wasylishen (University of Alberta) "High-Field NMR Studies of Strontium-87 in Solids"

13:50-14:15 Brandon Greer (University of Manitoba) "Characterisation of Chromium-bearing "Yellow Phase" in Model Nuclear Waste Glasses by Multinuclear Magnetic Resonance Spectroscopy"

14:15-14:40 Venkataraman Thangadurai (University of Calgary) "Evaluation of Structure, Ion-Exchange and Transport Properties of Fast Li ion Conducting Garnet-type Solid Electrolytes by Solid State Li NMR Spectroscopy and AC Impedance"

14:40-15:00 Coffee Break

Session 2 (CTCC, Chinook 4), Chair Scott Kroeker (University of Manitoba)

15:00-15:25 Robin Stein (Bruker Canada) "Proton Solid-State NMR Crystallography"

15:25-15:50 Frédéric Perras (University of Ottawa) "35Cl Solid-State NMR of Covalently-Bound, Organic, Chlorine at 21.1 T and the use of QUEST (QUadrupolar Exact SofTware)"

15:50-16:15Bryan Lucier (University of Windsor) "Solid-State NMR Investigations of 'Stacked' Square-Planar Pt(II) Systems"

16:15-16:40 Andreas Brinkmann (NRC Canada) "Dipolar Recoupling in Fast Magic-Angle-Spinning NMR at High Magnetic Fields"

16:40-17:05 Gillian Goward (McMaster University) "Measuring Ion Dynamics by NMR Observations from the Point of View of the Host Lattice"

17:10 Reception sponsored by Bruker Canada


NMR paper in Nature Chemistry (May 15/12)

V.N. Vukotic, K.J. Harris, K. Zhu, R.W. Schurko and S.J. Loeb, "Metal–organic frameworks with dynamic interlocked components," Nature Chemistry
(2012) online. http://dx.doi.org/10.1038/nchem.1354


Spring 2012

"Canadian NMR Research" News Bulletin (May 14/12)

Spring 2012 issue of the "Canadian NMR Research" news bulletin is now available for download.

You are welcome to share it with your colleagues and students.

Thanks for reading!



Recognition: Anthony Mittermaier (May 10/12)

Dr. Anthony Mittermaier, associate professor of chemistry at McGill University (Montreal), receives the 2012 Agilent Early Career Professor Award. The Agilent Early Career Professor Award is presented annually to recognize and encourage excellence in measurement research. Prof. Mittermaier has been awarded for his pioneering research in molecular biology, mutagenesis and NMR to study structure of proteins, their dynamics and function.

To read the press release by Agilent:
http://www.agilent.com/about/newsroom/presrel/2012/10may-ca12031.html


NMReady - 60 MHz bench-top NMR spectrometer (May 6/12)

contributed by Jackie Metropolit (Nanalysis Corp., Calgary, Alberta)


Nanalysis Corp. a Calgary based company has recently launched a 60MHz bench-top NMR spectrometer called the NMReady™. The Alberta Company was established in 2009 with a mandate to design and manufacture compact Nuclear Magnetic Resonance (NMR) devices. The company initially sought to commercialize Force-detected NMR (FDNMR) as realized in BOOMERANG technology, but soon transitioned to miniaturize traditional NMR to bring FT NMR technology to the bench or glovebox.
NMReady 60MHz bench-top NMR spectrometer

The NMReady™ debuted in March, 2012 at the American Chemical Society meeting in San Diego. Conference attendees were pleasantly surprised to find 60MHz spectroscopic resolution, running both 19F and 1H, at a fraction of the size and cost of current NMR instrumentation. The small size of the instrument allows it to fit on the benchtop, in the fume hood or even inside a glovebox. It comes equipped with a built-in touch screen display that features an easy-to-use, OneTouch NMR, operator interface. The NMReady is a cryogen-free NMR system, uses standard 3mm and 5 mm NMR tubes and has a very modest service schedule.

The NMReady has application in all types of industries, including oil & gas, chemical, pharma, biotech, and food processing, and in government and university labs. It also works as an ideal training tool in an academic setting, allowing students to gain hands-on experience with NMR. The compact NMR spectrometer can improve workflow, reduce costs of outsourcing and allow large organizations to optimize all of their spectroscopic resources.

Introduction to the NMReady 60P on YouTube

Nanalysis has just entered into a collaborative research agreement with Thesis Chemistry, a Green Chemistry organization in Cambridge, Ontario. The company will integrate the analytical capability of the NMReady bench-top NMR spectrometer into their program of transforming lignocellulosic biomass into green chemicals. See the press release at
http://www.accesswire.com/viewarticle.aspx?id=397349

Nanalysis will be showcasing the NMReady at CSC 2012, May 26-30, 2012, in Calgary. Visit booth #222, to get a live demo and see first-hand the capabilities of the NMReady.

For more information on the applications and functions of the NMReady, visit http://www.nanalysis.com
NMReady 60MHz bench-top NMR spectrometer

Recognition: Julian Zhu (April 29/12)

Polymer Chemistry (RSC) profiles Prof. Julian Zhu (Université de Montréal) as the author of the week.
http://blogs.rsc.org/py/2012/04/27/author-of-the-week-julian-zhu/


NMR paper in Science (April 19/12)

P. Neudecker, P. Robustelli, A. Cavalli, P. Walsh, P. Lundström, A. Zarrine-Afsar, S. Sharpe, M. Vendruscolo, and L.E. Kay, "Structure of an Intermediate State in Protein Folding and Aggregation," Science 336 (2012) 362-366. http://dx.doi.org/10.1126/science.1214203


Science Perspective: David Eliezer, "Visualizing Amyloid Assembly," Science 336 (2012) 308-309. http://dx.doi.org/10.1126/science.1220356


Physics of MRI: A Primer (April 13/12)

Physics of MRI: A Primer

An introductory lecture on physics of MRI by Donald Plewes and Walter Kucharczyk (University of Toronto).

D.B. Plewes and W. Kucharczyk,
"Physics of MRI: A Primer," Journal of Magnetic Resonance Imaging 35 (2012) 1038–1054. (Review: MR Physics for Clinicians) http://dx.doi.org/10.1002/jmri.23642

 
7th Solid-State NMR Workshop at CSC 2012 (updated April 30/12)

The National Ultrahigh-Field NMR Facility for Solids and Bruker Canada are pleased to present the 7th Annual Solid-State NMR Workshop at the 95th Canadian Chemistry Conference and Exhibition in Calgary (CSC 2012). The workshop will take place on Saturday, May 26, 2012, 13:00 - 19:00, in the Calgary TELUS Convention Centre.

This annual Canadian solid-state NMR event focuses on the latest developments in solid-state NMR spectroscopy with emphasis on practical aspects and applications in materials and life sciences. The workshop will be of interest not only to NMR spectroscopists, but also to students and other researchers interested in using modern NMR techniques in their research practice.

The workshop registration is free but the space is limited. To register please send your name and affiliation to Victor.Terskikh@nrc-cnrc.gc.ca

Please note, that the NMR workshop registration is separate from CSC 2012 registration.

Workshop program

Session 1, Chair David Bryce (University of Ottawa)

13:00-13:05 David Bryce (University of Ottawa) Opening comments

13:05-13:25 Anne-Marie Thompson (NSERC) "Major Resources Support program" (brief presentation and discussion)

13:25-13:50 Roderick Wasylishen (University of Alberta) "High-Field NMR Studies of Strontium-87 in Solids"

13:50-14:15 Brandon Greer (University of Manitoba) "Characterisation of chromium-bearing "yellow phase" in model nuclear waste glasses by multinuclear magnetic resonance spectroscopy"

14:15-14:40 Venkataraman Thangadurai (University of Calgary) "Evaluation of Structure, Ion-Exchange and Transport Properties of Fast Li ion Conducting Garnet-type Solid Electrolytes by Solid State Li NMR Spectroscopy and AC Impedance"

14:40-15:00 Coffee Break

Session 2, Chair Scott Kroeker (University of Manitoba)

15:00-15:25 Robin Stein (Bruker Canada) "Proton Solid-State NMR Crystallography"

15:25-15:50 Frédéric Perras (University of Ottawa) "35Cl Solid-State NMR of Covalently-Bound, Organic, Chlorine at 21.1 T and the use of QUEST (QUadrupolar Exact SofTware)"

15:50-16:15 Bryan Lucier (University of Windsor) "Solid-State NMR Investigations of 'Stacked' Square-Planar Pt(II) Systems"

16:15-16:40 Andreas Brinkmann (NRC Canada) "Dipolar Recoupling in Fast Magic-Angle-Spinning NMR at High Magnetic Fields"

16:40-17:05 Gillian Goward (McMaster University) "Measuring Ion Dynamics by NMR Observations from the Point of View of the Host Lattice"

17:10 Reception sponsored by Bruker Canada


IV Ibero-American NMR Meeting (April 4/12)

Dear Colleagues,

We cordially invite you to participate in the IV Ibero-American NMR Meeting which will be celebrated along with the VI GERMN Bienal Meeting and the III Iberian NMR Meeting, at the University of Aveiro, Portugal, from 25 to 28 September, 2012. This special arrangement will offer the Ibero-American NMR spectroscopists and others interested, a large audience and a great opportunity to present and share their results.

Registrations are open and abstracts to be considered for oral contribution can be submitted until April 30th.

Confirmed speakers:

Brian Goodfellow (CICECO, Aveiro, Portugal)
Claudio Fernandez (UNR, Rosario, Argentina)
Claudio Tormena (IQM, UNICAMP, Campinas Brazil)
Luis Alberto Colnago (EMBRAPA, Brasília, Brazil
Hartmut Oschkinat (FMP, Berlin, Germany)
Jarbas Resende (UFMG, Belo Horizonte, Brazil)
Jesús Angulo (CSIC, Seville, Spain)
João Rocha (CICECO, Aveiro, Portugal)
Marta Bruix (CSIC, Madrid, Spain)
Natàlia Carulla (IRB, Barcelona, Spain)
Julien Wist (Universidade del Valle, Cali, Colombia)
Volker Dötsch (Goethe Univ. Frankfurt, Germany)
IV Ibero-American NMR Meeting

Travel stipends: http://www.spq.pt/eventos/iberoanmr2012/?ver=travel

For full details, important deadlines and updates, please visit our website:
http://www.spq.pt/eventos/iberoanmr2012/

Looking forward to meet you in Aveiro,

The organizing committee


Cover article in Chemical Science (April 3/12)

Potent inhibition of ice recrystallization by low molecular weight carbohydrate-based surfactants and hydrogelators


C.J. Capicciotti, M. Leclère, F.A. Perras, D. Bryce, H. Paulin, J. Harden, Y. Liu and R.N. Ben,
"Potent inhibition of ice recrystallization by low molecular weight carbohydrate-based surfactants and hydrogelators," Chem. Sci. 3 (2012) 1408-1416. (Cover Article) http://dx.doi.org/10.1039/C2SC00885H

 
3rd Canadian Magnetism Meeting (April 2/12)

Dear colleagues,

The 3rd Canadian Magnetism Meeting will be held in Calgary on May 25th, right before the CSC kicks off. This day-long meeting is intended to allow researcher in all fields of magnetism to share their recent research developments, and network with other members of the Canadian magnetism community.

All interested are welcome to attend. In order to help organization, please send an email to confirm if you and your group will attend (contact information below).

We have a lineup of invited speakers covering various areas of magnetism: Daniel Gamelin (U Washington), Daniel Leznoff (SFU), Natia Frank (UVic), Laurie Thompson (MUN), TK Sham (Western), Kathryn Preuss (Guelph), and Arthur Mar (UofA).

There will be a poster session for students with best poster awards. We will be accepting email submissions of abstracts (200-word abstract, 1 picture) until May 7th.

There is no registration fee for this meeting.

More info can be found at:
http://www.chem.ucalgary.ca/research/groups/trudels/canadian-magnetism-meeting.html

Visit often, the website will get regular updates in the coming weeks.

All those interested to attend and/or to submit an abstract, please email Robin Arseneault at [raarsene "at" ucalgary.ca
]

We are looking forward to seeing all of you in Calgary.


NSERC awards $2.3 million for lithium ion battery research (March 22/12)

Gillian Goward (McMaster) is leading a major collaborative research project in lithium ion batteries which has been awarded a $2.3 million NSERC grant in the Automotive Partnership Canada program. The total value of this four years project is $3.5 million with contributions from industrial partners, GM Canada, Bruker Ltd., and Heka Electronics.

Researchers from McMaster include Prof. Gillian Goward, in electrochemistry and magnetic resonance, Prof. Gianluigi Botton, in electron microscopy, and Prof. Bartek Protas, in mathematical modeling. Prof. Janine Mauzeroll at McGill provides expertise in scanning electrochemical microscopy, and two electrochemistry groups lead by Prof. Andy Sun at the University of Western Ontario, and Prof. Steen Schougaard at the Université du Québec à Montréal.

For more about this project:

$3.5 million partnership to jumpstart confidence in lithium ion car batteries (McMaster Daily News)

Gillian Goward Gets $3.5m for Electric Car Battery Research (C&CB, McMaster)

McMaster gets $3.5m jolt for electric car battery research (Hamilton Spectator)

Bringing Minds to Market: Government of Canada Invests in Auto Innovation (NSERC news release, March 20, 2012)



Solid-State NMR in Materials for Energy Storage and Conversion (March 21/12)

A special issue of Solid State Nuclear Magnetic Resonance guest-edited by Clare Grey (Cambridge) and Gillian Goward (McMaster), Volume 42, Pages 1-98 (April 2012)
http://www.sciencedirect.com/science/journal/09262040/42

Editorial

Clare P. Grey, Gillian R. Goward, Editorial "Solid-State NMR in Materials for Energy Storage and Conversion," Solid State Nuclear Magnetic Resonance
42 (2012) 1. http://dx.doi.org/10.1016/j.ssnmr.2012.03.001

Canadian contributions

A. Kuhn, M. Kunze, P. Sreeraj, H.-D. Wiemhöfer, V. Thangadurai, M. Wilkening, P. Heitjans, "NMR relaxometry as a versatile tool to study Li dynamics in potential battery materials," Solid State Nuclear Magnetic Resonance 42 (2012) 2-8. http://dx.doi.org/10.1016/j.ssnmr.2012.02.001

L.J.M. Davis, X.J. He, A.D. Bain, G.R. Goward, "Studies of Lithium Ion Dynamics in Paramagnetic Cathode Materials Using 6Li 1D Selective Inversion Methods," Solid State Nuclear Magnetic Resonance 42 (2012) 26-32. http://dx.doi.org/10.1016/j.ssnmr.2012.01.002


NMR paper in Angewandte Chemie (March 14/12)

Frédéric A. Perras and David L. Bryce, "Direct Investigation of Covalently Bound Chlorine in Organic Compounds by Solid-State 35Cl NMR Spectroscopy and Exact Spectral Line-Shape Simulations," Angew. Chem. Int. Ed. (2012) online. http://dx.doi.org/10.1002/anie.201200728

This is a second publication in Angewandte Chemie featuring results 900obtained using resources of the National Ultrahigh-Field NMR Facility for Solids. See the complete list of research publications enabled by the Facility here (complete list).


54th Rocky Mountain Conference on Analytical Chemistry (March 1/12)

The 54th Rocky Mountain Conference on Analytical Chemistry is taking place July 15-19, 2012 at the Copper Conference Center in Copper Mountain, Colorado. This year's conference will feature the 35th International EPR Symposium, as well as the world-renowned Solid-State NMR Symposium.

Abstracts are now being accepted for both oral and poster presentations. Deadline to submit an oral presentation abstract is May 1, 2012. Deadline to submit a poster presentation abstract is June 15, 2012. For information on submitting an abstract visit
http://www.rockychem.com/conference/call-for-abstracts.html

Conference registration is now open. Discounts are offered to those who are registered and paid on or before July 1, 2012
http://www.rockychem.com/conference/registration.html

You can access additional details on hotel reservations, discounted travel, area attractions and program content at http://www.rockychem.com


New NMR book (March 1/12)

Axelson
Solid State Nuclear Magnetic Resonance: A Practical Introduction (Volume 1)

David E. Axelson (author)
Paperback: 472 pages
Publisher: CreateSpace (January 26, 2012)
Language: English
ISBN: 978-1469982274
http://www.amazon.com/dp/1469982277

"Solid state nuclear magnetic resonance now offers a wide variety of methods for characterization of materials of different compositions over a wide range of experimental conditions (temperatures, pressures, etc.). Both simple and sophisticated pulse sequences enable one to selectively probe and quantify physical properties of interest. This book mainly dwells on the practical aspects of selected topics and uses a largely non-mathematical, although extensively referenced, approach to the introduction of solid state NMR concepts."

Chapter 1 : Principles of Solid State NMR
Chapter 2 : Introduction to Pulse Sequences
Chapter 3 : Decoupling
Chapter 4 : Quantitative Analysis
Chapter 5 : Artifacts
Chapter 6 : Line Broadening Mechanisms
Chapter 7 : Resolution Enhancement
Chapter 8 : Variable Temperature

For the detailed table of contents
http://www.chemometrics-analysis.com/SSNMR.html

To contact the author, Dr. David E. Axelson
http://www.chemometrics-analysis.com/


CCSB 2012 (March 1/12)

We are pleased to announce the 2nd China Canada Systems Biology Conference and the 19th Methods in Protein Structure Analysis, which will take place at the Ottawa Convention Centre, Ottawa, Canada from June 25-28, 2012. The 2012 symposium is being organized and hosted by the Ottawa Institute of Systems Biology (University of Ottawa), The International Association for Protein Structure Analysis and Proteomics, and the China-Ontario BioAnalytic Consortium (COBAC).

The goal of this meeting is to bring together internationally recognized scientists and students in the field of systems biology, protein biochemistry, and proteomics to promote scientific discussion and the development of new collaborations.

Of special interest for NMR spectroscopists will be the session "Dynamic links between protein structure and function". Invited speakers to this session include Lewis Kay (University of Toronto), Katherine Henzler-Wildman (Washington University School of Medicine), Gianluigi Veglia (University of Minnesota), Kevin Gardner (University of Texas Southwestern) and Dorothee Kern (Brandeis).

More information can be found at http://www.oisb.ca/june_2012_symposium/ccsb_2012.htm

Registration is now open. Abstract submission deadline is May 15th, 2012.

Natalie Goto

Associate Professor

Department of Chemistry
University of Ottawa
10 Marie Curie
Ottawa, ON, K1N 6N5

email: Natalie.Goto "at" uottawa.ca
Tel (613) 562-5800 (6918)
Fax (613) 562-5170
Web: http://mysite.science.uottawa.ca/ngoto/Welcome.html


NANUC 2012 Biomolecular NMR BootCamp (update March 6/12)

NANUC 2012 Biomolecular NMR BootCamp will be hosted by the NMR Facility in Chemistry at the University of Toronto, June 4th to 9th, 2012 on campus.

Our keynote lecturer this year is Prof. Chad Reinstra (UIUC) on BioSolids NMR. We will have Dr. Frank Delaglio (NIDDK, NIH) for the NMRPipe Suite; Dr. Nico Tjandra (LBPC, NIH) with Dynamics and Relaxation; Dr. Bruce Johnson (UMBC) on NMRView; Dr. Charles Schwieters (ISL, NIH) demonstrating Xplor-NIH, and one day on pulse sequence programming (Agilent/Bruker).

For more information visit
http://www.nanuc.ca/nmrbootcamp/2012_NMR_BootCamp/Welcome.html

Please mark your calendars,

Tim
--
Timothy Burrow, Ph.D. MBA
Manager, NMR
University of Toronto 416-978-5728

NMR News!
http://nmrweb.chem.utoronto.ca:8084/users/timburrow/
NMR Web pages:
http://www.chem.utoronto.ca/facilities/nmr/nmr.html


Solid-State NMR Symposium at CSC 2012 (March 1/12)

Colleagues,

this is a reminder that the CSC 2012 abstract submission deadline is February 15.

On behalf of the organizing committee for the 95th Canadian Chemistry Conference and Exhibition, it is my pleasure to invite you to take part in the "Solid-State NMR" symposium sponsored by the Physical, Theoretical and Computational Division of the Chemical Society of Canada. CSC 2012 will be held in Calgary, May 26-30, 2012. Three half-day sessions will be devoted to the Solid-State NMR symposium tentatively beginning Sunday afternoon, May 27th.

The confirmed invited speakers are Michèle Auger (Laval), Jochen Autscbach (SUNY - Buffalo), Alex Bain (McMaster), Darren Brouwer (Redeemer), David Bryce (Ottawa), Gillian Goward (McMaster), Yining Huang (Western), Scott Kroeker (Manitoba), Andrew MacFarlane (UBC), Karl T. Mueller (PNNL - Richland), Luke O'Dell (NRC Canada), John Ripmeester (NRC Canada), Rob Schurko (Windsor), Victor Terskikh (NRC Canada), Gang Wu (Queen's).

In addition, the conference will feature the usual poster session. Finally, on Saturday, May 26th the National Ultrahigh-Field NMR Facility for Solids and Bruker Canada will be hosting the 7th Annual Solid-State NMR Workshop. I certainly hope that you and your colleagues can attend the workshop.

Please visit the conference web site http://www.csc2012.ca for a full list of symposia and for abstract submission instructions. All abstracts must be submitted on-line by Wednesday, February 15. The Web site also provides information on the many attractions in the Calgary area.

I am looking forward to seeing you in Calgary at the end of May. Very best wishes.

Yours sincerely,

Rod

--
Dr. Roderick E. Wasylishen
Canada Research Chair in Physical Chemistry
Department of Chemistry
Gunning/Lemieux Chemistry Centre
University of Alberta
Edmonton, Alberta
Canada T6G 2G2

Tel: 1-780-492-4336
Lab: 1-780-492-5732
Web: http://ramsey.chem.ualberta.ca